US 7,462,464 B1
Method for the detection of antimicrobial residues in food and bodily fluid samples
Pieter Cornelis Langeveld, Delft (Netherlands); Jacobus Stark, Rotterdam (Netherlands); and Petrus Andreas Van Paridon, Voorburg (Netherlands)
Assigned to DSM IP Assets B.V., (Netherlands)
Appl. No. 10/89,874
PCT Filed Oct. 03, 2000, PCT No. PCT/EP00/09874
§ 371(c)(1), (2), (4) Date Sep. 03, 2002,
PCT Pub. No. WO01/25471, PCT Pub. Date Apr. 12, 2001.
Claims priority of application No. 99203264 (EP), filed on Oct. 04, 1999; and application No. 99203429 (EP), filed on Oct. 18, 1999.
This patent is subject to a terminal disclaimer.
Int. Cl. C12Q 1/18 (2006.01); C12Q 1/02 (2006.01); C12N 1/20 (2006.01)
U.S. Cl. 435—32  [435/29; 435/252.5; 435/253.4] 16 Claims
 
1. A process for determining the presence or absence of an antimicrobial residue in a sample, which process comprises:
(i) contacting the sample with a test suitable for determining the presence or absence of an antimicrobial residue in the sample;
(ii) inactivating any natural disturbing compound present in the sample which is capable of inhibiting the test and which leads to a false positive result absent said inactivating step, by heating said contacted sample and test to a temperature of 75° C. to 85° C. for a sufficient time interval to inactivate the natural disturbing compound that may be present in the sample; followed by
(iii) incubating the contacted sample and test to determine whether microbial growth occurs, whereby the absence of microbial growth indicates the presence of at least one antimicrobial residue.