US 7,459,030 B2
Manufacturing method of Nb3Sn superconductive wire using powder technique
Takayoshi Miyazaki, Kobe (Japan); Hiroyuki Kato, Kobe (Japan); Kyoji Zaitsu, Kobe (Japan); and Kyoji Tachikawa, Hiratsuka (Japan)
Assigned to Kabushiki Kaisha Kobe Seiko Sho, Hyogo (Japan)
Appl. No. 11/596,470
PCT Filed May 17, 2005, PCT No. PCT/JP2005/008970
§ 371(c)(1), (2), (4) Date Nov. 13, 2006,
PCT Pub. No. WO2005/117032, PCT Pub. Date Dec. 08, 2005.
Claims priority of application No. 2004-155254 (JP), filed on May 25, 2004.
Prior Publication US 2007/0175543 A1, Aug. 02, 2007
Int. Cl. H01L 39/24 (2006.01)
U.S. Cl. 148—98  [419/23; 29/599] 9 Claims
OG exemplary drawing
 
1. A manufacturing method of an Nb3Sn superconductive wire using a powder technique, the method comprising the steps of:
reducing oxygen in primary particles of at least one of metallic powders selected from Ta powder and Nb powder using Na, Mg, or Ca;
aggregating the primary particles thereby obtaining secondary particles in a shape of coral;
filling, as a raw powder, an intermetallic compound powder obtained from said secondary particles and Sn powder, or a mixture of the secondary particles and the Sn powder, into a sheath made of Nb or an Nb based alloy;
performing a diameter-reduction process on the sheath to form a wire;
heat treating the wire; and
forming a superconductive layer on the interface between the sheath and the filled powder.