US 7,589,141 B2
Organic-inorganic polymer composites and their preparation by liquid infusion
Michael A. Zalich, Pittsburgh, Pa. (US); Gregory J. McCollum, Gibsonia, Pa. (US); and Thomas G. Rukavina, New Kensington, Pa. (US)
Assigned to PPG Industries Ohio, Inc., Cleveland, Ohio (US)
Filed on Dec. 14, 2006, as Appl. No. 11/610,651.
Prior Publication US 2008/0146716 A1, Jun. 19, 2008
Int. Cl. C08L 75/04 (2006.01); C08K 3/20 (2006.01)
U.S. Cl. 524—430  [524/590] 12 Claims
 
1. A method of forming a composite of an inorganic-thermoset polymer comprising:
(a) contacting the thermoset polymer with a solution of the precursor of the inorganic particulate phase so as to swell the thermoset polymer
(b) infusing the precursor into the surface region of the thermoset polymer and
(c) subjecting the infused precursor to conditions sufficient to form an inorganic particulate phase having a particle size less than 1000 nanometers dispersed in the thermoset polymer phase.