US 7,579,591 B2
Method and apparatus for analyzing sample
Masaru Takakura, Tokyo (Japan)
Assigned to Jeol Ltd., Tokyo (Japan)
Filed on Nov. 13, 2007, as Appl. No. 11/939,235.
Claims priority of application No. 2006-307592 (JP), filed on Nov. 14, 2006.
Prior Publication US 2008/0111072 A1, May 15, 2008
Int. Cl. H01J 37/26 (2006.01); G01N 23/223 (2006.01); G01N 23/00 (2006.01)
U.S. Cl. 250—310  [250/306; 250/307; 250/492.2; 378/46] 5 Claims
OG exemplary drawing
 
1. A method of analyzing a sample by irradiating the sample with an electron beam, spectrally dispersing and detecting characteristic X-rays emanating from the sample in response to the irradiation by a wavelength-dispersive X-ray spectrometer, and measuring intensities of the characteristic X-rays at positions where characteristic X-ray peaks are detected,
wherein background intensities of the characteristic X-rays at the positions where the characteristic X-ray peaks are detected are found based on a mean atomic number calculated using values derived by quantitative analysis based on the intensities of the characteristic X-rays measured by an energy-dispersive X-ray spectrometer at corresponding analysis positions on the sample, and
wherein the background intensities are subtracted from the peak intensities at the positions where the characteristic X-ray peaks are detected by the wavelength-dispersive X-ray spectrometer, thus finding net characteristic X-ray intensities.