US 7,547,405 B2
Solid state deformation processing of crosslinked high molecular weight polymeric materials
David Wayne Schroeder, Winona Lake, Ind. (US); Jordan H. Freedman, Fort Wayne, Ind. (US); James E. Gunter, Claypool, Ind. (US); Brian D. Salyer, East Warsaw, Ind. (US); and H. Gene Hawkins, Warsaw, Ind. (US)
Assigned to Biomet Manufacturing Corp., Warsaw, Ind. (US)
Filed on Apr. 12, 2006, as Appl. No. 11/402,561.
Application 11/402561 is a continuation in part of application No. 10/963974, filed on Oct. 13, 2004, granted, now 7,344,672.
Application 10/963974 is a continuation in part of application No. 10/963975, filed on Oct. 13, 2004.
Claims priority of provisional application 60/616811, filed on Oct. 07, 2004.
Prior Publication US 2006/0258767 A1, Nov. 16, 2006
Int. Cl. C08J 5/00 (2006.01); B28B 3/00 (2006.01); B28B 3/26 (2006.01); B29C 43/02 (2006.01); B29C 43/32 (2006.01)
U.S. Cl. 264—319  [264/320; 264/331.19; 264/331.21; 264/331.11; 264/331.17] 25 Claims
OG exemplary drawing
 
1. A method for reducing the free radical concentration in irradiated crosslinked bulk polymer, the polymer being in the form of a bulk material elongated in an axial direction, the method comprising:
heating the crosslinked bulk material to a compression deformable temperature;
applying a force to deform the heated bulk material in a direction orthogonal to the axial direction by extruding the heated bulk material through an isoareal die; and
cooling the polymer to a solidification temperature.