US 7,531,132 B1
Chemical and biological warfare agent decontaminating methods using dioxirane producing formulations
Carrie A. Delcomyn, Lynn Haven, Fla. (US); Jean Renard, Panama City, Fla. (US); William Wallace, Panama City, Fla. (US); and Michael Henley, Panama City, Fla. (US)
Assigned to Applied Research Associates, Inc., Albuquerque, N. Mex. (US)
Filed on Jun. 06, 2006, as Appl. No. 11/422,504.
Application 11/422504 is a division of application No. 10/687864, filed on Oct. 17, 2003.
Int. Cl. A61L 2/18 (2006.01); C11D 1/00 (2006.01); C11D 3/10 (2006.01); C11D 3/20 (2006.01); C11D 3/39 (2006.01); C11D 3/43 (2006.01)
U.S. Cl. 422—28  [510/372; 510/383; 510/505; 510/506; 510/509] 22 Claims
 
1. A method of decontaminating materials contaminated with chemical or biological warfare agents consisting of the steps of:
preparing a first solution consisting of water, one or more monopersulfate compounds, and one or more buffers selected from the group consisting of alkali metal salts of bicarbonate and carbonate; and
preparing a second solution consisting of one or more ketones, at least one of said ketones being selected from the group consisting of acetone, 2-butanone, 2-pentanone, 2-hydroxy-4-methyl-2-pentanone, hexafluoroacetone, trifluoroacetone, acetophenone, camphorsulfonic acid, and levulinic acid, wherein the first solution and the second solution are separately contained;
forming a decontaminating composition having a pH of from 5 to about 9, by mixing said first solution and said second solution to achieve in situ generation of dioxirane in the composition; and
contacting said composition with materials contaminated by chemical or biological warfare agents.